USA - MILWAUKEE
Metallurgical Associates, Inc.
2325-B Parklawn Drive
Waukesha, WI 53186
Phone: (262) 798-8098
Fax: (262) 798-8099
Toll Free: (800) 798-4966
info@metassoc.com

Technical Articles

Material Characteristics, Analytical Techniques, and Process and Failure Analysis

graphic element

9/18/2009 When “In Spec” Doesn’t Work (9/18/2009)
6/20/2008 Biological Corrosion of Metals (6/20/2008)
3/20/2008 Fatigue Failure (3/20/2008)
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9/18/2009 When “In Spec” Doesn’t Work 9/18/2009
Failed Axle Shaft
The axle shaft was specified to be made from SAE 4140 alloy steel. The elements, their percentages, and the results of chemical analysis of the axle are shown below:

 Percent of Element
ElementShaftSAE 4140
Carbon0.450.38-0.45
Manganese0.960.75-1.00
Sulfur0.0260.040 Max.
Phosporus0.0110.035 Max.
Silicon0.170.15-0.35
Chromium0.990.80-1.10
Molybdenum0.200.15-0.25

One of the first questions that must be answered in any failure analysis is "Was the part made from the specified material?" If the answer is "yes", the analyst may be tempted to go off in another direction in search of the cause of a failure. Our recent analysis of a failed axle shaft demonstrates that a more careful evaluation is prudent even when the chemical analysis is "in spec".

By any criteria the shaft was within specification. However, the carbon is at the maximum specified value, manganese is near the maximum specified value and chromium is in the upper third of the specified range. The maximum or near maximum values of this combination of elements, although within specification, result in a higher than typical hardenability when this material is heat treated. The result of this higher than typical hardenability was an unacceptable percentage of quench cracks during a heat treating procedure that had been used successfully in the past on axle shafts with more typical SAE 4140 chemistries. Many of these cracked axle shafts were placed in service, resulting in short term failures.

Optical Photomicrograph of Polished Cross Section through Cracked Axle Shaft
Optical photomicrograph of polished cross section through the cracked axle shaft. 40X

Metallurgical Associates is in the business of solving problems, in both service failures and manufacturing process problems. We don't actively pursue the routine testing market in chemical analysis and tensile testing. However, many clients call on us to provide these services because of the "value added" analysis we provide by reviewing "routine" test results with an eye towards the processing and service they will be subjected to. As a result, we often recommend a change in material or tightening of the material specifications. This often provides a significant savings "up front" before processing or service failure costs are incurred.

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